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The method usually adopted for estimating the peptonizing power of pepsina porci consists in dissolving 1 to 2 grains in 8 to 12 ounces of water, to which 40 to 60 minims of hydrochloric acid has been added. 500 to 1,000 grains of hard-boiled white of egg, granulated by rubbing through a wire sieve, is immersed in the liquid, and the whole kept at 98° to 130° F. for four hours, when the undissolved albumen is filtered off through muslin, and, after partial drying, is weighed to ascertain the amount dissolved.
A little snow, which had fallen in the course of the last two or three days, now remained upon the land, lightly powdering the higher parts, especially those having a northern aspect, and creating a much more wintry sensation than the large broad patches or drifts, which, on all tolerably high land in these regions, remain undissolved during the whole of each successive summer.
The Burgesses declared his answer unsatisfactory. They demanded a specific acknowledgment that the House remained undissolved. Mathews and the Council finally agreed to revoke the declaration of dissolution, but still insisted on referring the dispute to the Lord Protector.
M. de Valicours furnishes us with the best method for preparing this mixture: "Into a bottle of the capacity of about two ounces, pour thirty or forty drops of bromine, the precise quantity not being of importance. Then add, grain by grain, as much iodine as the bromine will dissolve till quite saturated. This point is ascertained when some grains of the iodine remain undissolved.
At the bottom was a modicum of white powder, undissolved. I poured the tea into the cup again then a second time into the saucer. This time nothing remained and I proceeded to pour cream into the saucer, until it was filled. Madam watched me with distended eyes, and trembling from head to foot. Then suddenly she uttered a cry a movement of mine had caused the cry.
The mean of several, which I made, was 86 degrees 30 minutes. Professor Miller states that these crystals, when reduced to a fine powder, are soluble in hydrochloric acid, leaving some undissolved silex behind; the addition of oxalate of ammonia gives a copious precipitate of lime.
Daintree found that a piece of undissolved gold in a bottle containing chloride of gold in solution had, owing to a portion of the cork having fallen into the liquid, grown or accretionised so much that it could not be extracted through the neck. This lead Mr. Charles Wilkinson, who has contributed much to our scientific knowledge of metallurgy, to experiment further in the same direction.
The total carbon was found to be: "cold-rolled," 1.108 per cent.; hardened, 1.128 per cent.; and annealed, 0.924 and 0.860 per cent. Some of the disks were submitted to the action of an oxidizing solution consisting of a cold saturated solution of potassium bichromate with 5 per cent. by volume of pure concentrated sulphuric acid. In all cases a blackish magnetic residue was left undissolved.
So that by treatment with chromic acid in the cold nearly the whole of the carbon remains undissolved with the cold-rolled and annealed disks, but only about one-sixth of the total carbon is left undissolved in the case of the hardened disk. The authors then give a resume of previous work on the subject.
It is essential that the solution should be cold and that the stannous chloride should not be present in great excess, otherwise a secondary reaction takes place, resulting in the reduction of the mercurous chloride to metallic mercury: SnCl + 2HgCl > SnCl + 2Hg. Heat at a temperature just below boiling until the undissolved residue is white or until solvent action has ceased.
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