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Updated: May 10, 2025
Lavoisier proposed to test these suppositions by calcining a weighed quantity of tin in a closed glass vessel, which had been weighed before, and should be weighed after, the calcination.
Boyle supposed that the increase in weight which accompanies the calcination of a metal is due to the fixation of "matter of fire" by the calcining metal; Rey regarded the increase in weight as the result of the combination of the air with the metal; Mayow thought that the atmosphere contains two different kinds of "airs," and one of these unites with the heated metal.
The results were these: there was no change in the total weight of the apparatus and its contents; when the vessel was opened after the calcination was finished, air rushed in, and the whole apparatus now weighed more than it did before the vessel was opened; the weight of the air which rushed in was exactly equal to the increase in the weight of the tin produced by the calcination, in other words, the weight of the inrushing air was exactly equal to the difference between the weights of the tin and the calx formed by calcining the tin.
Calcination of the Ore. Having arranged a proper mixture of ores in the yard, it is weighed out in boxes to the calcining-men. This is drawn up an inclined plane over the tops of the furnaces, and from thence emptied through hoppers, 3-1/2 to 4-1/2 tons at a time, into the large calcining furnace.
The principal point about this mode of treatment is the squeezing out of the mercury, whereby the amalgam goes into the retort in the form of powder, thus preventing the slagging of the iron and enclosure of the gold. The second point of importance is thorough calcining before smelting.
The alchemist acted as a sort of conscience to the metals, minerals, salts, and other substances he submitted to the processes of his laboratory. He treated them as a wise physician might treat an ignorant and somewhat refractory patient. "I know what you want better than you do," he seems often to be saying to the metals he is calcining, separating, joining and subliming.
We have seen how the experiment of burning or calcining such a metal as lead "destroyed" the lead as such, leaving an entirely different substance in its place, and how the original metal could be restored by the addition of wheat to the calcined product. To the alchemist this was "mortification" and "revivification" of the metal.
He would perhaps have had a rheumatic patient wrapped in the skin of a wolf or a wild cat, and in case of a malignant fever with "purples" or petechiae, or of an obstinate king's evil, he might have prescribed a certain black powder, which had been made by calcining toads in an earthen pot; a choice remedy, taken internally, or applied to any outward grief.
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