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The nitrate of soda varies in purity in different parts, and often contains nodules of common salt. According to Mr. Blake, the proportion of nitrate of soda varies from 20 to 75 per cent. An analysis by Mr. A. Hayes, of an average specimen, gave: Nitrate of Soda.... 64.98 Sulphate of Soda.... 3.00 Chloride of Soda... 28.69 Iodic Salts......... 0.63 Shells and Marl..... 2.60 99.90
Concentrate the solution of meconic acid, allow a portion to crystallize, and apply tests. Tests. Morphine and its acetate give an orange-red colour with nitric acid, becoming brighter on standing; decompose iodic acid, setting free iodine; with perchloride of iron, gives a rich indigo-blue; with bichromate of potassium, a green turning to brown.
The "mother-water" at some of the refineries is very rich in iodic salts, and is supposed to contain much muriate of lime. T. Reeks has ascertained that the muriate of lime is very abundant.
With respect to the origin of this saline mass, from the manner in which the gently inclined, compact bed follows for so many miles the sinuous margin of the plain, there can be no doubt that it was deposited from a sheet of water: from the fragments of embedded shells, from the abundant iodic salts, from the superficial saliferous crust occurring at a higher level and being probably of marine origin, and from the plain resembling in form those of Chile and that of Uspallata, there can be little doubt that this sheet of water was, at least originally, connected with the sea.
When the alkaloid is heated in a watchglass with a drop of strong sulphuric acid until the acid begins to fume, and is then allowed to get quite cold, a drop of nitric acid produces a brilliant red colour. The iodic acid test is very delicate, but requires great care, and may be used in the presence of organic matter.
It lies close beneath the surface, and follows for a length of one hundred and fifty miles the margin of a grand basin or plain; this, from its outline, manifestly must once have been a lake, or more probably an inland arm of the sea, as may be inferred from the presence of iodic salts in the saline stratum. The surface of the plain is 3300 feet above the Pacific.
Reeks has analysed for me some of the salt from the salina near the Rio Negro; he finds it composed entirely of chloride of sodium, with the exception of 0.26 of sulphate of lime and of 0.22 of earthy matter: there are no traces of iodic salts. Some salt from the salina Chiquitos, in the Pampean formation, is equally pure.
It lies close beneath the surface, and follows for a length of one hundred and fifty miles the margin of a grand basin or plain; this, from its outline, manifestly must once have been a lake, or more probably an inland arm of the sea, as may be inferred from the presence of iodic salts in the saline stratum. The surface of the plain is 3300 feet above the Pacific. 19th.
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