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Updated: May 13, 2025
Of the methods of precipitating the compounds of the protoxide and estimating the acid, that of the phosphate is by far the most accurate, titrating with uranium solution; 99.82 is a nearly constant average with me, much depending on the operator's familiarity with the uranium process. The methods of Lenssen, or ferricyanide of potassium method, yields very widely differing results.
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